Experiments in Organic Chemistry:  A Challenge Oriented Approach
For student text, please visit:  http://murov.info/orglab.htm  

Instructor's Manual Table of Contents with hotlinks

 
  Description Page http://murov.info/orglab.htm  
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Table of Contents     iii I-1-Itoc.pdf
       
Experiment 1   SOLVENT POLARITY AND MISCIBILITY 1 I-2-E01-6.pdf
Experiment 2   RECRYSTALLIZATION: PURIFICATION OF SOLIDS 3 I-2-E01-6.pdf
Experiment 3  MELTING POINTS AND RANGES   5 I-2-E01-6.pdf
Experiment 4  WÖHLER'S UREA SYNTHESIS   7 I-2-E01-6.pdf
Experiment 5  SAPONIFICATION USING REFLUX   9 I-2-E01-6.pdf
Experiment 6  EXTRACTION: A SEPARATION AND PURIFICATION TECHNIQUE   11 I-2-E01-6.pdf
       
Experiment 7  IDENTIFICATION OF AN ORGANIC UNKNOWN. I  13 I-3-E07-11.pdf
Experiment 8  SIMPLE AND FRACTIONAL DISTILLATION   15 I-3-E07-11.pdf
Experiment 9  PAPER AND COLUMN CHROMATOGRAPHY   17 I-3-E07-11.pdf
Experiment 10  IDENTIFICATION OF AN ORGANIC UNKNOWN. II   19 I-3-E07-11.pdf
Experiment 11 VACUUM DISTILLATION, POLYMERIZATION OF STYRENE   21 I-3-E07-11.pdf
       
Experiment 12  BROMINATION OF CINNAMIC ACID   23 I-4-E12-16.pdf
Experiment 13  FERMENTATION OF SUCROSE   25 I-4-E12-16.pdf
Experiment 14  HYDRATION OF ALKENES   27 I-4-E12-16.pdf
Experiment 15  NUCLEOPHILIC SUBSTITUTION   29 I-4-E12-16.pdf
Experiment 16  ELIMINATION REACTIONS   31 I-4-E12-16.pdf
Experiment 17  NUCLEOPHILIC SUBSTITUTION WITH SACCHARIN   33 I-5-E17-21.pdf
Experiment 18  STEREOCHEMISTRY OF NUCLEOPHILIC SUBSTITUTION   35 I-5-E17-21.pdf
Experiment 19  REDUCTION WITH NaBH4: STERIC AND CONJUGATION EFFECTS   37 I-5-E17-21.pdf
Experiment 20  GRIGNARD SYNTHESIS   39 I-5-E17-21.pdf
Experiment 21  ELECTROPHILIC AROMATIC SUBSTITUTION  41 I-5-E17-21.pdf
       
Experiment 22  FISCHER ESTERIFICATION   43 I-6-E22-27.pdf
Experiment 23  TAUTOMERISM OF 2,4-PENTANEDIONE   45 I-6-E22-27.pdf
Experiment 24 A DOUBLE ALDOL CONDENSATION   47 I-6-E22-27.pdf
Experiment 25 IDENTIFICATION OF LIQUID AND SOLID UNKNOWNS   49 I-6-E22-27.pdf
Experiment 26  MULTISTEP SYNTHESIS   51 I-6-E22-27.pdf
Experiment 27  ANALYSIS OF A CARBOHYDRATE   53 I-6-E22-27.pdf
       
Experiment 28  DIELS-ALDER REACTION   55 I-7-E28-34.pdf
Experiment 29  MICROWAVE REACTIONS: A RESEARCH PROJECT   57 I-7-E28-34.pdf
Experiment 30  SYNTHESIS AND USE OF A DYE   59 I-7-E28-34.pdf
Experiment 31  SOME POLYMER EXPERIMENTS   61 I-7-E28-34.pdf
Experiment 32  SYNTHESIS OF A TRIBOLUMINESCENT COMPOUND   63 I-7-E28-34.pdf
Experiment 33  STEAM DISTILLATION: SEPARATION OF BIOACTIVE MOLECULES   65 I-7-E28-34.pdf
Experiment 34  A FATTY ACID FROM NUTMEG   67 I-7-E28-34.pdf
       
Experiment 35  ACIDITY OF BENZOIC ACIDS: A LINEAR FREE ENERGY GRAPH   69 I-8-E35-41.pdf
Experiment 36  A GREEN WITTIG REACTION   71 I-8-E35-41.pdf
Experiment 37   ACID CATALYSIS   73 I-8-E35-41.pdf
Experiment 38  ENANTIOMERS OF IBUPROFEN   75 I-8-E35-41.pdf
Experiment 39  SYNTHESIS OF COPPER(II) GYLCINATE  77 I-8-E35-41.pdf
Experiment 40  ALKYL PARABENS: SYNTHESIS AND DETECTION IN COSMETICS   79 I-8-E35-41.pdf
Experiment 41  SYNTHESIS AND TESTING OF ANTIBIOTICS   81 I-8-E35-41.pdf
       
EXERCISES     password not needed
Exercise 1  Review of General Chemistry   83 I-9-X1-2.pdf
Exercise 2  Lewis Structures, Isomers, Bond Polarity, Molecular Models and Geometry   95 I-9-X1-2.pdf
       
Exercise 3  Chemical Toxicity Considerations  99 I-10-X3-5.pdf
Exercise 4  Group Frequencies in Infrared Spectra  101 I-10-X3-5.pdf
Exercise 5  Identification of Unknowns   103 I-10-X3-5.pdf
       
Exercise 6  Structure - Activity Relationships: Acidity and pKa Values  107 I-11-X6-8.pdf
Exercise 7  Choosing Laboratory Procedures   109 I-11-X6-8.pdf
Exercise 8  Mechanisms of Reactions   111 I-11-X6-8.pdf
       
Exercise 9  Petrochemicals and Climate   113 I-12-X9-11.pdf
Exercise 10  Solvents   115 I-12-X9-11.pdf
Exercise 11  Energies in Perspective   117 I-12-X9-11.pdf
       
Exercise 12  Controversial Chemicals: Issues and Synthesis   119 I-13-X12-14.pdf
Exercise 13  Material Selection   121 I-13-X12-14.pdf
Exercise 14  Thought Provoking Problems   123 I-13-X12-14.pdf
       
Exercise 15  Preparation of a Key for Reaction-Map of Organic Chemistry   125 I-14-X15.pdf
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