Experiments in Organic
Chemistry: A Challenge Oriented Approach
For student text, please visit:
http://murov.info/orglab.htm
Instructor's Manual Table of Contents with hotlinks
| Description | Page |
http://murov.info/orglab.htm password needed |
|
| Table of Contents | iii | I-1-Itoc.pdf | |
| Experiment 1 | SOLVENT POLARITY AND MISCIBILITY | 1 | I-2-E01-6.pdf |
| Experiment 2 | RECRYSTALLIZATION: PURIFICATION OF SOLIDS | 3 | I-2-E01-6.pdf |
| Experiment 3 | MELTING POINTS AND RANGES | 5 | I-2-E01-6.pdf |
| Experiment 4 | WÖHLER'S UREA SYNTHESIS | 7 | I-2-E01-6.pdf |
| Experiment 5 | SAPONIFICATION USING REFLUX | 9 | I-2-E01-6.pdf |
| Experiment 6 | EXTRACTION: A SEPARATION AND PURIFICATION TECHNIQUE | 11 | I-2-E01-6.pdf |
| Experiment 7 | IDENTIFICATION OF AN ORGANIC UNKNOWN. I | 13 | I-3-E07-11.pdf |
| Experiment 8 | SIMPLE AND FRACTIONAL DISTILLATION | 15 | I-3-E07-11.pdf |
| Experiment 9 | PAPER AND COLUMN CHROMATOGRAPHY | 17 | I-3-E07-11.pdf |
| Experiment 10 | IDENTIFICATION OF AN ORGANIC UNKNOWN. II | 19 | I-3-E07-11.pdf |
| Experiment 11 | VACUUM DISTILLATION, POLYMERIZATION OF STYRENE | 21 | I-3-E07-11.pdf |
| Experiment 12 | BROMINATION OF CINNAMIC ACID | 23 | I-4-E12-16.pdf |
| Experiment 13 | FERMENTATION OF SUCROSE | 25 | I-4-E12-16.pdf |
| Experiment 14 | HYDRATION OF ALKENES | 27 | I-4-E12-16.pdf |
| Experiment 15 | NUCLEOPHILIC SUBSTITUTION | 29 | I-4-E12-16.pdf |
| Experiment 16 | ELIMINATION REACTIONS | 31 | I-4-E12-16.pdf |
| Experiment 17 | NUCLEOPHILIC SUBSTITUTION WITH SACCHARIN | 33 | I-5-E17-21.pdf |
| Experiment 18 | STEREOCHEMISTRY OF NUCLEOPHILIC SUBSTITUTION | 35 | I-5-E17-21.pdf |
| Experiment 19 | REDUCTION WITH NaBH4: STERIC AND CONJUGATION EFFECTS | 37 | I-5-E17-21.pdf |
| Experiment 20 | GRIGNARD SYNTHESIS | 39 | I-5-E17-21.pdf |
| Experiment 21 | ELECTROPHILIC AROMATIC SUBSTITUTION | 41 | I-5-E17-21.pdf |
| Experiment 22 | FISCHER ESTERIFICATION | 43 | I-6-E22-27.pdf |
| Experiment 23 | TAUTOMERISM OF 2,4-PENTANEDIONE | 45 | I-6-E22-27.pdf |
| Experiment 24 | A DOUBLE ALDOL CONDENSATION | 47 | I-6-E22-27.pdf |
| Experiment 25 | IDENTIFICATION OF LIQUID AND SOLID UNKNOWNS | 49 | I-6-E22-27.pdf |
| Experiment 26 | MULTISTEP SYNTHESIS | 51 | I-6-E22-27.pdf |
| Experiment 27 | ANALYSIS OF A CARBOHYDRATE | 53 | I-6-E22-27.pdf |
| Experiment 28 | DIELS-ALDER REACTION | 55 | I-7-E28-34.pdf |
| Experiment 29 | MICROWAVE REACTIONS: A RESEARCH PROJECT | 57 | I-7-E28-34.pdf |
| Experiment 30 | SYNTHESIS AND USE OF A DYE | 59 | I-7-E28-34.pdf |
| Experiment 31 | SOME POLYMER EXPERIMENTS | 61 | I-7-E28-34.pdf |
| Experiment 32 | SYNTHESIS OF A TRIBOLUMINESCENT COMPOUND | 63 | I-7-E28-34.pdf |
| Experiment 33 | STEAM DISTILLATION: SEPARATION OF BIOACTIVE MOLECULES | 65 | I-7-E28-34.pdf |
| Experiment 34 | A FATTY ACID FROM NUTMEG | 67 | I-7-E28-34.pdf |
| Experiment 35 | ACIDITY OF BENZOIC ACIDS: A LINEAR FREE ENERGY GRAPH | 69 | I-8-E35-41.pdf |
| Experiment 36 | A GREEN WITTIG REACTION | 71 | I-8-E35-41.pdf |
| Experiment 37 | ACID CATALYSIS | 73 | I-8-E35-41.pdf |
| Experiment 38 | ENANTIOMERS OF IBUPROFEN | 75 | I-8-E35-41.pdf |
| Experiment 39 | SYNTHESIS OF COPPER(II) GYLCINATE | 77 | I-8-E35-41.pdf |
| Experiment 40 | ALKYL PARABENS: SYNTHESIS AND DETECTION IN COSMETICS | 79 | I-8-E35-41.pdf |
| Experiment 41 | SYNTHESIS AND TESTING OF ANTIBIOTICS | 81 | I-8-E35-41.pdf |
| EXERCISES | password not needed | ||
| Exercise 1 | Review of General Chemistry | 83 | I-9-X1-2.pdf |
| Exercise 2 | Lewis Structures, Isomers, Bond Polarity, Molecular Models and Geometry | 95 | I-9-X1-2.pdf |
| Exercise 3 | Chemical Toxicity Considerations | 99 | I-10-X3-5.pdf |
| Exercise 4 | Group Frequencies in Infrared Spectra | 101 | I-10-X3-5.pdf |
| Exercise 5 | Identification of Unknowns | 103 | I-10-X3-5.pdf |
| Exercise 6 | Structure - Activity Relationships: Acidity and pKa Values | 107 | I-11-X6-8.pdf |
| Exercise 7 | Choosing Laboratory Procedures | 109 | I-11-X6-8.pdf |
| Exercise 8 | Mechanisms of Reactions | 111 | I-11-X6-8.pdf |
| Exercise 9 | Petrochemicals and Climate | 113 | I-12-X9-11.pdf |
| Exercise 10 | Solvents | 115 | I-12-X9-11.pdf |
| Exercise 11 | Energies in Perspective | 117 | I-12-X9-11.pdf |
| Exercise 12 | Controversial Chemicals: Issues and Synthesis | 119 | I-13-X12-14.pdf |
| Exercise 13 | Material Selection | 121 | I-13-X12-14.pdf |
| Exercise 14 | Thought Provoking Problems | 123 | I-13-X12-14.pdf |
| Exercise 15 | Preparation of a Key for Reaction-Map of Organic Chemistry | 125 | I-14-X15.pdf |